Structure Elucidation by Modern Nmr : A Workbook (3 REV UPD)

During the last few years, routine applications of NMR techniques have been further developed. Spectrometers of the latest generation offer new types of experiments, such as spinlock and inverse-detected methods. In this third, revised and expanded edition, new methodology is introduced and incorporated into new exercises. In addition, a new chapter has been introduced which demonstrates the fully detailed interpretation of two typical examples. Introduction.- Methodology.- High Magnetic Fields. One-dimensional 1H,1H Correlation. Two-Dimensional 1H,13C One-Bond Correlation. Two-Dimensional 1H,13C Long-Range Correlation. NOE Experiments. 13C,13C-Correlation.- Two Demonstration Examples. Rearrangement of a Benzothiazepine to a Benzothiazole Derivative. Structure Elucidation of a Triterpene Saponin.- Exercises.- Strategies.- Solutions.